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1 article(s) from Berton, Mateo

Disposable cartridge concept for the on-demand synthesis of turbo Grignards, Knochel–Hauser amides, and magnesium alkoxides

Mateo Berton,
Kevin Sheehan,
Andrea Adamo and
D. Tyler McQuade

Beilstein J. Org. Chem. 2020, 16, 1343–1356, doi:10.3762/bjoc.16.115

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Graphical Abstract

Figure 1: Comparing on-demand coffee and turbo Grignard pod-style machines.

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Figure 2: Ranking of the 20 most cited Grignard reagents (SciFinder March 26, 2019).

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Figure 3: On-demand prototype. A) Inside view of the pump with a flexible bag containing a yellow liquid layi...

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Figure 4: Temperature evolution measured with thermocouples along the column outer surface at three different...

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Figure 5: Stratified bicomponent column (Diba Omnifit EZ Solvent Plus) composed of magnesium (chips/powder, 1...

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Scheme 1: Continuous flow synthesis of TMPMgCl⋅LiCl with a stratified packed-bed column of activated magnesiu...

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Scheme 2: Continuous flow synthesis of TMPMgCl⋅LiBr with a stratified packed-bed column of activated magnesiu...

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Scheme 3: Continuous flow synthesis of t-AmylOMgCl⋅LiCl with a stratified packed-bed column of activated magn...

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Figure 6: Steady-state concentration stability during the conversion of iPrCl in THF (56 mL, 2.2 M) into iPrM...

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Scheme 4: Synthesis of iPrMgCl⋅LiCl on the ODR prototype.

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Scheme 5: Synthesis of HMDSMgCl⋅LiCl on the ODR prototype.

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Published 19 Jun 2020

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